Title :

Ethyl 4,6-dimethyl-3-oxo-2-phenyl-3,7-dihydro-2H-pyrazolo[3,4-b]pyridine-5-carboxylate monohydrate

Author(s) :

Akhramez, Soufiane [Auteur]
Université Sultan Moulay Slimane [USMS ]
Hafid, Abderrafia [Auteur]
Université Sultan Moulay Slimane [USMS ]
Khouili, Mostafa [Auteur]
Université Sultan Moulay Slimane [USMS ]
Mentre, Olivier [Auteur]
Unité de Catalyse et Chimie du Solide - UMR 8181 [UCCS]
Ketatni, El Mostafa [Auteur]
Université Sultan Moulay Slimane [USMS ]

Journal title :

IUCrData

Volume number :

1

Publication date :

2016-10

HAL domain(s) :

Chimie/Chimie inorganique

English abstract : [en]

In the title compound, C17H17N3O3·H2O, the dihedral angle between the 4,6-dimethyl-pyrazolo­[3,4-b]pyridine-3-one unit [maximum deviation = 0.048 (2) Å] and the phenyl ring is 5.1 (1)°. The structure is characterized by ...
Show more >In the title compound, C17H17N3O3·H2O, the dihedral angle between the 4,6-dimethyl-pyrazolo­[3,4-b]pyridine-3-one unit [maximum deviation = 0.048 (2) Å] and the phenyl ring is 5.1 (1)°. The structure is characterized by disorder of the carboxyl­ate O atoms, which are split into two parts with a major component of 0.898 (4). In the crystal, the organic mol­ecules and lattice water mol­ecules are linked via O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds. The mol­ecules are also linked by C—H⋯π and weak offset π–π stacking inter­actions, forming sheets parallel to (001).Show less >

Language :

Anglais

Audience :

Internationale

Popular science :

Non

Administrative institution(s) :

ENSCL
CNRS
Centrale Lille
Univ. Artois
Université de Lille

Collections :

• Unité de Catalyse et Chimie du Solide (UCCS) - UMR 8181

Research team(s) :

Matériaux inorganiques, structures, systèmes et propriétés (MISSP)

Submission date :

2019-09-25T14:05:59Z
2024-04-23T12:08:15Z