Multiscale investigation of the crystallization ...
Document type :
Article dans une revue scientifique
Permalink :
Title :
Multiscale investigation of the crystallization mechanisms and solute redistribution during annealing of a Fe64B24Y4Nb6Al0.4 metallic glass
Author(s) :
Avettand-Fènoël, Marie-Noëlle [Auteur]
Unité Matériaux et Transformations (UMET) - UMR 8207
Sauvage, Xavier [Auteur]
Groupe de physique des matériaux [GPM]
Université de Rouen Normandie [UNIROUEN]
Marinova, Maya [Auteur]
Institut Chevreul - FR2638
Addad, Ahmed [Auteur]
Unité Matériaux et Transformations (UMET) - UMR 8207
Unité Matériaux et Transformations (UMET) - UMR 8207
Sauvage, Xavier [Auteur]
Groupe de physique des matériaux [GPM]
Université de Rouen Normandie [UNIROUEN]
Marinova, Maya [Auteur]
Institut Chevreul - FR2638
Addad, Ahmed [Auteur]
Unité Matériaux et Transformations (UMET) - UMR 8207
Journal title :
Journal of Alloys and Compounds
Abbreviated title :
Journal of Alloys and Compounds
Volume number :
887
Pages :
161264
Publisher :
Elsevier BV
Publication date :
2021-12
ISSN :
0925-8388
English keyword(s) :
A. Fe based metallic glass
Primary crystallization
Atom probe tomography
D. transmission electron microscopy
D. X-ray diffractometry
Primary crystallization
Atom probe tomography
D. transmission electron microscopy
D. X-ray diffractometry
HAL domain(s) :
Chimie/Matériaux
English abstract : [en]
The mechanisms and the sequence of crystallization of a Fe64B24Y4Nb6Al0.4 metallic glass were investigated experimentally. To this end, the microstructure of the metallic glass after interrupted isothermal treatments at a ...
Show more >The mechanisms and the sequence of crystallization of a Fe64B24Y4Nb6Al0.4 metallic glass were investigated experimentally. To this end, the microstructure of the metallic glass after interrupted isothermal treatments at a temperature between glass transition and primary crystallization was studied by complementary techniques, namely atom probe tomography, transmission electron microscopy and X-ray diffractometry. During the early stages of crystallization of the glass, some nanometric (Fe,Nb)B crystals nucleate first by rejecting Y at their interface, which hinders their growth. The Fe62B14Y3 dendritic phase starts growing in a second step. Longer annealings lead to the development of chemical gradients in the amorphous matrix surrounding Fe62B14Y3 crystals, which favors the nucleation of additional nanometric (Fe,Nb)2.4B crystals.Show less >
Show more >The mechanisms and the sequence of crystallization of a Fe64B24Y4Nb6Al0.4 metallic glass were investigated experimentally. To this end, the microstructure of the metallic glass after interrupted isothermal treatments at a temperature between glass transition and primary crystallization was studied by complementary techniques, namely atom probe tomography, transmission electron microscopy and X-ray diffractometry. During the early stages of crystallization of the glass, some nanometric (Fe,Nb)B crystals nucleate first by rejecting Y at their interface, which hinders their growth. The Fe62B14Y3 dendritic phase starts growing in a second step. Longer annealings lead to the development of chemical gradients in the amorphous matrix surrounding Fe62B14Y3 crystals, which favors the nucleation of additional nanometric (Fe,Nb)2.4B crystals.Show less >
Language :
Anglais
Audience :
Internationale
Popular science :
Non
Administrative institution(s) :
Université de Lille
CNRS
INRA
ENSCL
CNRS
INRA
ENSCL
Collections :
Submission date :
2021-08-30T10:26:57Z
2021-09-01T06:21:16Z
2021-09-01T06:21:16Z