Titre :

ToF-SIMS analyses of brittle crack initiation of T91 steel by liquid sodium

Auteur(s) :

Hamdane, Ouadie [Auteur]
Unité Matériaux et Transformations - UMR 8207 [UMET]
Vogt, Jean-Bernard [Auteur]
Unité Matériaux et Transformations - UMR 8207 [UMET]
Proriol Serre, Ingrid [Auteur]
Unité Matériaux et Transformations - UMR 8207 [UMET]
Nuns, Nicolas [Auteur]
Unité de Catalyse et Chimie du Solide - UMR 8181 [UCCS]

Titre de la revue :

Materials Chemistry and Physics

Numéro :

145

Pagination :

243-249

Date de publication :

2014

Mot(s)-clé(s) en anglais :

Metals
Secondary ion mass spectroscopy (SMS)
Mechanical properties
Embrittlement

Discipline(s) HAL :

Chimie/Matériaux
Physique [physics]/Matière Condensée [cond-mat]/Science des matériaux [cond-mat.mtrl-sci]

Résumé en anglais : [en]

Tempering the martensitic T91 steel at 550 °C instead of 750 °C (recommended heat treatment) makes T91 more sensitive to liquid metal embrittlement. Especially, in liquid sodium, T91 tempered at 550 °C exhibited a brittle ...
Lire la suite >Tempering the martensitic T91 steel at 550 °C instead of 750 °C (recommended heat treatment) makes T91 more sensitive to liquid metal embrittlement. Especially, in liquid sodium, T91 tempered at 550 °C exhibited a brittle fracture while it was ductile in air. Liquid sodium initiated an intergranular crack which then propagated by transgranular mode in the bulk of the specimen. ToF-SIMS analyses were performed on dedicated Small Punch Test specimens in order to distinguish the contribution of the mechanical loading from the sodium environment. Controlled elastic or plastic deformations on pre immersed (503 °C during 169 h) and on as received materials were performed in liquid sodium at 450 °C. Sodium penetration at prior austenitic grains boundaries and at laths boundaries has been pointed out by TOF-SIMS. It is concluded that the sodium penetration requires plastic deformation.Lire moins >

Langue :

Anglais

Audience :

Internationale

Vulgarisation :

Non

Établissement(s) :

Université de Lille
ENSCL
CNRS
Centrale Lille
INRA
Univ. Artois

Collections :

• Unité Matériaux et Transformations (UMET) - UMR 8207

Équipe(s) de recherche :

Métallurgie Physique et Génie des Matériaux

Date de dépôt :

2019-05-16T16:45:10Z
2020-12-07T08:22:53Z
2020-12-07T08:23:49Z