Titre :

Optimization of cold plasma process parameters for organosilicon films deposition on carbon steel: Study of the surface pretreatment effect on corrosion protection performance in 3-wt% NaCl medium

Auteur(s) :

Esbayou, M. [Auteur]
Bentiss, Fouad [Auteur]
Casetta, Mathilde [Auteur]
Unité Matériaux et Transformations - UMR 8207 [UMET]
Nyassi, Abdelhamid [Auteur]
Jama, charafeddine [Auteur]
Unité Matériaux et Transformations - UMR 8207 [UMET]

Titre de la revue :

Journal of Alloys and Compounds

Numéro :

758

Pagination :

148-161

Date de publication :

2018

Discipline(s) HAL :

Sciences de l'ingénieur [physics]/Matériaux
Sciences de l'ingénieur [physics]/Génie des procédés
Chimie/Matériaux
Chimie/Polymères

Résumé en anglais : [en]

Organosilicon films were deposited on carbon steel using plasma enhanced chemical vapour deposition (PECVD) process prepared from cold plasma polymerization of 1,1,3,3-tetramethyldisiloxane (TMDSO). The experimental design ...
Lire la suite >Organosilicon films were deposited on carbon steel using plasma enhanced chemical vapour deposition (PECVD) process prepared from cold plasma polymerization of 1,1,3,3-tetramethyldisiloxane (TMDSO). The experimental design technique allowed determining the optimal conditions of the plasma process. The effect of different surface pretreatments was investigated using amorphous phosphatation, argon (Ar) and nitrogen (N2) plasma. Coatings showing a hydrophobic character and good adhesion were obtained. Several surface characterization techniques using Fourier transform infrared spectroscopy (FTIR), nuclear magnetic resonance (NMR), scanning electron microscopy (SEM), contact angle, cross-cut and surface profilometry were used. The protection efficiency against corrosion of the deposited films has been demonstrated by coupling different electrochemical techniques such as open circuit potential (OCP) and electrochemical impedance spectroscopy (EIS) in 3 wt% NaCl solution. The organosilicon coatings showed good barrier against corrosion even after long immersion time in the aggressive environment, especially when N2 plasma pretreatment is performed.Lire moins >

Langue :

Anglais

Audience :

Internationale

Vulgarisation :

Non

Établissement(s) :

Université de Lille
ENSCL
CNRS
INRA

Collections :

• Unité Matériaux et Transformations (UMET) - UMR 8207

Équipe(s) de recherche :

Ingénierie des Systèmes Polymères

Date de dépôt :

2019-05-17T09:25:12Z
2023-12-19T16:26:02Z