Titre :

Hadamard NMR spectroscopy in solids

Auteur(s) :

Ashida, J. [Auteur]
Kupce, E. [Auteur]
Amoureux, Jean-Paul [Auteur]

Titre de la revue :

J. Magn. Reson.

Nom court de la revue :

J. Magn. Reson.

Pagination :

129-135

Date de publication :

2006-01

ISSN :

1090-7807

Mot(s)-clé(s) en anglais :

solid-state NMR
fast multi-dimensional spectra
Hadamard
dipolar assisted rotational resonance
HETCOR
proton driven spin diffusion

Discipline(s) HAL :

Chimie

Résumé en anglais : [en]

The duration of 2D and 3D NMR experiments in solids can be reduced by several orders of magnitude by using frequency domain Hadamard encoding with long selective pulses. We demonstrate Hadamard encoded experiments in 13C ...
Lire la suite >The duration of 2D and 3D NMR experiments in solids can be reduced by several orders of magnitude by using frequency domain Hadamard encoding with long selective pulses. We demonstrate Hadamard encoded experiments in 13C enriched solids samples. To avoid multiple quantum interferences, the Hadamard encoding pulses are applied sequentially rather than simultaneously in this study. Among other possible applications, dipolar assisted rotational resonance experiments and measurement of NOESY type build-up rates in proton driven spin diffusion are demonstrated.Lire moins >

Langue :

Anglais

Établissement(s) :

Université de Lille
CNRS
Centrale Lille
ENSCL
Univ. Artois

Collections :

• Unité de Catalyse et Chimie du Solide (UCCS) - UMR 8181

Équipe(s) de recherche :

RMN et matériaux inorganiques (RM2I)

Date de dépôt :

2023-05-30T18:34:50Z